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Book
xix, 959 pages : illustrations (some color) ; 29 cm
  • 1. Introduction. Section I: MEASUREMENT BASICS. 2. Electrical Components and Circuits. 3. Operational Amplifiers in Chemical Instrumentation. 4. Digital Electronics and Computers. 5. Signals and Noise. Instrumental Analysis in Action: The Electronic Analytical Laboratory. Section II: ATOMIC SPECTROSCOPY. 6. An Introduction to Spectrometric Methods. 7. Components of Optical Instruments. 8. An Introduction to Optical Atomic Spectrometry. 9. Atomic Absorption and Atomic Fluorescence Spectrometry. 10. Atomic Emission Spectrometry. 11. Atomic Mass Spectrometry. 12. Atomic X-Ray Spectrometry. Instrumental Analysis in Action: Monitoring Mercury. Section III: MOLECULAR SPECTROSCOPY. 13. An Introduction to Ultraviolet-Visible Molecular Absorption Spectrometry. 14. Applications of Ultraviolet-Visible Molecular Absorption Spectrometry. 15. Molecular Luminescence Spectrometry. 16. An Introduction to Infrared Spectrometry. 17. Applications of Infrared Spectrometry. 18. Raman Spectroscopy. 19. Nuclear Magnetic Resonance Spectroscopy. 20. Molecular Mass Spectrometry. 21. Surface Characterization by Spectroscopy and Microscopy. Instrumental Analysis in Action: Assessing the Authenticity of the Vinland Map: Surface Analysis in the Service of History, Art, and Forensics. Section IV: ELECTROANALYTICAL CHEMISTRY. 22. An Introduction to Electroanalytical Chemistry. 23. Potentiometry. 24. Coulometry. 25. Voltammetry. Instrumental Analysis in Action: Measuring the Parts to Understand the Whole: The Microphysiometer. Section V: SEPARATION METHODS. 26. An Introduction to Chromatographic Separations. 27. Gas Chromatography. 28. High-Performance Liquid Chromatography. 29. Supercritical Fluid Chromatography and Extraction. 30. Capillary Electrophoresis, Electrochromatography, and Field-Flow Fractionation. Instrumental Analysis in Action: The Bisphenol A Controversy. Section VI: MISCELLANEOUS METHODS. 31. Thermal Methods. 32. Radiochemical Methods. 33. Automated Methods of Analysis. 34. Particle Size Determination. Instrumental Analysis in Action: The John F. Kennedy Assassination. Appendices. Appendix 1: Evaluation of Analytical Data. Appendix 2: Activity Coefficients. Appendix 3: Some Standard and Formal Electrode Potentials. Appendix 4: Compounds Recommended for the Preparation of Standard Solutions of Some Common Elements. Answers to Selected Problems. Index.
  • (source: Nielsen Book Data)9781305577213 20170515
PRINCIPLES OF INSTRUMENTAL ANALYSIS is the standard for courses on the principles and applications of modern analytical instruments. In the 7th edition, authors Skoog, Holler, and Crouch infuse their popular text with updated techniques and new Instrumental Analysis in Action case studies. Updated material enhances the book's proven approach, which places an emphasis on the fundamental principles of operation for each type of instrument, its optimal area of application, its sensitivity, its precision, and its limitations. The text also introduces students to elementary analog and digital electronics, computers, and the treatment of analytical data. A companion website is available, providing students with tutorials on instrumental methods, Excel files of data analysis, and simulations of analytical techniques to help them visualize important concepts. Digital Object Identifiers (DOIs) are provided for most references to the primary literature.
(source: Nielsen Book Data)9781305577213 20170515
Science Library (Li and Ma)
CHEM-174-01, CHEM-274-01
Book
xvi, 683 p. : ill ; 25 cm.
  • Introduction-- BASIC ASPECTS OF ELECTROCHEMISTRY-- Fundamentals of Electrode Reactions-- Voltammetric Techniques-- Softwares able to assist Electrochemistry-- PRACTICAL ASPECTS-- Basic Equipment for Electrochemical Measurements-- APPLICATIVE ASPECTS-- The Electrochemical Behaviour of First Row Transition Metal Sandwich Complexes: Metallocenes and Metallacarboranesl-- The Electrochemical Behaviour of Transition Metal Complexes-- Metal Complexes Containing Redox Active Ligands-- Electrochemistry and Molecular Reorganizations-- The Reactivity of Transition Metal Complexes with Small Molecules-- Transition Metal Clusters-- The "Direct" Electrochemistry of Redox-Active Proteins-- Single-Molecule Electronics: from Molecular Metal Wires to Molecular Motors Spectroelectrochemistry-- An Introduction to Electrogenerated-- Chemiluminescence-- Appendices.
  • (source: Nielsen Book Data)9781849730716 20160608
In order to understand the basic aspects of an electrochemical investigation on inorganic molecules (in its widest meaning, of any molecule which contains at least one metal centre) it must be taken into account that in these molecules the metal-ligand bonds are of the prevailingly covalent type. Since electrochemical techniques allow you to add or remove electrons in a controlled manner, it is conceivable that the addition or removal of electrons inside these molecules can lead to the formation of new bonds or to the breakage of existing bonds. The main aim of this book is to study the effects of such electron addition and removal processes on the molecular frames. The second edition of this classic book has been fully revised and updated and is a straightforward, logical introduction to electrochemical investigations for inorganic chemists. All chapters have been rewritten with new material including: - the addition of reactivity with nitric oxide to the chapter on the reactivity of metal complexes with small molecules - thiolate-protected gold nanoclusters has been added to the chapter on metal-sulfur and metal-carbonyl clusters - a new chapter on the digital simulation of electrochemical responses - a new chapter on the theoretical calculations to explain the nature of the electrochemical activity of metal complexes - new chapters on spectroelectrochemistry and electrochemiluminescence. The book covers every aspect of inorganic electrochemistry - the introduction is followed by chapters on the basic aspects of electrochemistry followed by practical and applicative aspects and ends with full appendices. It is probably the only publication with a simple approach to electrochemical aspects of the topics in inorganic chemistry. Bridging the gap between undergraduate and research-level electrochemistry books, this publication will be a welcome addition to the literature of inorganic chemists. It will also be particularly useful to final year students in chemistry and as background reading for graduates and researchers without adequate electrochemical knowledge to become active in the discipline or who want to collaborate with electrochemists.
(source: Nielsen Book Data)9781849730716 20160608
Science Library (Li and Ma)
CHEM-174-01, CHEM-274-01
Book
xviii, 312 p. : ill. (some col.) ; 25 cm.
  • Porous Materials and Electrochemistry. Electrochemical Processes Involving Porous Materials. Electrocatalysis. Electrochemistry of Aluminosilicates. Electrochemistry of Metal-Organic Frameworks. Electrochemistry of Porous Oxides and Related Materials. Electrochemistry of Porous Carbons and Nanotubes. Electrochemistry of Porous Polymers and Hybrid Materials. Electrochemical Sensing via Porous Materials. Supercapacitors, Batteries, Fuel Cells, and Related Applications. Magnetoelectrochemistry and Photoelectrochemistry of Porous Materials. Microporous Materials in Electrosynthesis and Environmental Remediation. References. Index.
  • (source: Nielsen Book Data)9781439806333 20160528
Porous materials have attracted considerable attention in the last decades because of the wide variety of scientific and technological applications, such as catalysis, shape- and size-selective absorption and adsorption, gas storage, and electrode materials. This book focuses on generalized theoretical modeling and describes redox processes for different porous materials, assessing their electrochemical applications. To present a focused analysis, the author limits discussion to a selection of important porous materials considered relatively homogeneous, from an electrochemical point of view. These include porous silicates and aluminosilicates, metal oxides, polyoxometalates and related materials, metal-organic frameworks, porous carbons, carbon nanotubes and fullerenes, and several hybrid materials.
(source: Nielsen Book Data)9781439806333 20160528
Science Library (Li and Ma)
CHEM-174-01, CHEM-274-01

4. Solid state electrochemistry [2009 - 2011]

Book
2 v. : ill. ; 25 cm.
  • Preface FUNDAMENTALS, APPLICATIONS AND PERSPECTIVES OF SOLID STATE ELECTROCHEMISTRY - A SYNOPSIS Solid vs. Liquid State Thermodynamics and Kinetics of Charge Carriers Usefulness of Electrochemical Cells Materials Research Strategies: Bulk Defect Chemistry Materials Research Strategy: Boundary Defect Chemistry Nanoionics SUPERIONIC MATERIALS: STRUCTURAL ASPECTS Techniques Families of Superionic Conductors Current Status and Future Prospects DEFECT EQUILIBRIA IN SOLIDS AND RELATED PROPERTIES: AN INTRODUCTION Defect Structure of Solids: Thermodynamic Approach Basic Relationships between the Defect Equilibria and Charge Tranfer in Solids Examples of Functional Materials with Different Defect Structures ION-CONDUCTING NANOCRYSTALS: THEORY, METHODS AND APPLICATIONS Theoretical Aspects Applications and Perspectives Experimental Methods Review of the Current Experimental Data and their Agreement with Theory Overview and Areas for Future Development THE FUNDAMENTALS AND ADVANCES OF SOLID STATE ELECTROCHEMISTRY: INTERCALATION (INSERTION) AND DEINTERCALATAION (EXTRACTION) IN SOLID STATE ELECTRODES Thermodynamics of Intercalation and Deintercalation Kinetics of Intercalation and Deintercalation Methodological Overview SOLID STATE ELECTROCHEMICAL REACTIONS OF ELECTROACTIVE MICRO- AND NANOPARTICLES IN A LIQUID ELECTROLYTE ENVIRONMENT Methodological Aspects Theory Examples and Applications ALKALI METAL CATION AND PROTON CONDUCTORS: RELATIONSHIPS BETWEEN COMPOSITION, CRYSTAL STRUCTURE AND PROPERTIES Principles of Classification and General Comments Crystal-Chemistry Factors Affecting Cationic Conductivity Crystal Structural Screening and Studies of the Conduction Paths Conductors with Large Alkaline Ions Lithium Ion Conductors Proton Conductors CONDUCTING SOLIDS: IN THE SEARCH FOR MULTIVALENT CATION TRANSPORT Analysis of Trivalent Cation Transport Search for Tetravalent Cation Conductors OXYGEN ION-CONDUCTING MATERIALS Oxygen Ionic Transport in Acceptor-Doped Oxide Phases: Relevant Trends Stabilized Zirconia Electrolytes Doped Ceria Anion Conductors Based on Bi2O3 Transport Properties of Other Fluorite-Related Phases: Selected Examples Perovskite-Type LnBO3 (B=Ga, , Al, In, Sc, Y) and their Derivatives Perovskite-Related Mixed Conductors: A Short Overview La2Mo2O9-Based Electrolytes Solid Electrolytes with Apatite Structure POLYMER AND HYBRID MATERIALS, THEIR ELECTROCHEMISTRY AND APPLICATIONS Introduction Fundamentals Fluorinated Ionomer Membranes Non-Fluorinated Ionomer Membranes High Temperature PEMs Conclusion ELECTRONICALLY CONDUCTING POLYMERS Solid Organic and Inorganic Electrochemically Active Materials for Galvanic Cells Operating at Moderate Temperatures General Features of Doping-Induced Changes in Pi-Conjugated Polymers HIGH-TEMPERATURE APPLICATIONS OF SOLID ELECTROLYTES: GAS ANALYSIS, PUMPING AND CONVERSION Characteristics of a Current-Carrying Electrode on an Oxide Electrolyte Operating Modes Cell Materials Cell Designs Examples of Applications ELECTROCHEMICAL SENSORS: FUNDAMENTALS, KEY MATERIALS AND APPLICATIONS Operation Principles Materials Challenges Applications.
  • (source: Nielsen Book Data)9783527323180 20160528
The only comprehensive handbook on this important and rapidly developing topic combines fundamental information with a brief overview of recent advances in solid state electrochemistry, primarily targeting specialists working in this scientific field. Particular attention is focused on the most important developments performed during the last decade, methodological and theoretical aspects of solid state electrochemistry, as well as practical applications. The highly experienced editor has included chapters with critical reviews of theoretical approaches, experimental methods and modeling techniques, providing definitions and explaining relevant terminology as necessary. Several other chapters cover all the key groups of the ion-conducting solids important for practice, namely cationic, protonic, oxygen-anionic and mixed conductors, but also conducting polymer and hybrid materials. Finally, the whole is rounded off by brief surveys of advances in the fields of fuel cells, solid-state batteries, electrochemical sensors, and other applications of ion-conducting solids. Due to the very interdisciplinary nature of this topic, this is of great interest to material scientists, polymer chemists, physicists, and industrial scientists, too.
(source: Nielsen Book Data)9783527323180 20160528
Science Library (Li and Ma)
CHEM-174-01, CHEM-274-01
Book
xxi, 410 p. : ill. ; 25 cm.
Science Library (Li and Ma)
CHEM-174-01, CHEM-274-01
Book
xi, 1,039 p. : ill. ; 26 cm.
Science Library (Li and Ma)
CHEM-174-01, CHEM-274-01
Book
xviii, 485 p. : ill. ; 25 cm.
  • Preface.Chapter 1. Single Electron Transfer at an Electrode.1.1 Introduction.1.2 Cyclic Voltammetry of Fast Electron Transfers.1.3 Technical Aspects.1.4 Electron Transfer Kinetics.1.5 Successive One-Electron Transfers vs. Two-Electron Transfers.References and Notes.Chapter 2. Coupling of Electrode Electron Transfers with Homogeneous Chemical Reactions.2.1 Introduction.2.2 Establishing the Mechanisms and Measuring the Rate Constants for Homogeneous Reactions by Means of Cyclic Voltammetry and Potential Step Chronoamperometry.2.3 Application of Redox Catalysis to the Kinetic Characterization of Fast Follow-up Reactions.2.4 Product Distribution in Preparative Electrolysis.2.5 Chemical Classification and Examples.2.6 Redox Properties of Transient Radicals.2.7 Electrochemistry as a Trigger for Radical Chemistry or Ionic Chemistry.References and Notes.Chapter 3. Electron Transfer, Bond Breaking, and Bond Formation.3.1 Introduction.3.2 Dissociative Electron Transfer.3.3 Interactions Between Fragments in the Product Cluster.3.4 Stepwise vs. Concerted Mechanisms.3.5 Cleavage of Ion Radicals. Reactions of Radicals with Nucleophiles.3.6 Role of Solvent in Ion-radical Cleavage and in Stepwise vs. Concerted Competitions.3.7 Dichotomy and Connections between SN2 Reactions and Dissociative Electron Transfers.References and Notes.Chapter 4. Molecular catalysis of Electrochemical Reactions.4.1 Introduction.4.2 Homogeneous Molecular Catalysis.4.3 Supported Molecular catalysis (Immobilized catalysts).References and Notes.Chapter 5. Enzymatic Catalysis of Electrochemical Reactions.5.1 Introduction.5.2 Homogeneous Enzymatic Catalysis.5.3 Immobilized Enzymes in Monomolecular Layers.5.4 Spatially Ordered Multimonomolecular Layered Enzyme coatings.References and Notes.Chapter 6. Appendixes.6.1 Single Electron Transfer at an Electrode.6.2 Coupling of Homogeneous Chemical Reactions with Electron transfer.6.3 Electron Transfer, Bond Breaking, and Bond Formation.6.4 Analysis of Supported Molecular catalysis by Rotating Disk Electrode Voltammetry.6.5 Enzymatic catalysis Responses.References and Notes.Glossary of Symbols.Index.
  • (source: Nielsen Book Data)9780471445739 20160528
This book is based on the George Fisher Baker Lecture given by Jean Michel Saveant at Cornell University in Fall 2002. This is the first book focusing on molecular electrochemistry. It relates to other fields, including photochemistry and biochemistry. It outlines clearly the connection between concepts, experimental illustrations, proofs and supporting methods. It appendixes to provide rigorous demonstrations to prevent an overload of algebra in the main text. Applications are oriented, focused on analyzing the results obtained rather than the methodology.
(source: Nielsen Book Data)9780471445739 20160528
dx.doi.org Wiley Online Library
Science Library (Li and Ma)
CHEM-174-01, CHEM-274-01
Book
xiv, 346 p. : ill. ; 25 cm.
  • Preface. PART I: FUNDAMENTALS OF CHEMISTRY IN NON--AQUEOUS SOLUTIONS: ELECTROCHEMICAL ASPECTS. Properties of Solvents and Solvent Classification. Solvation and Complex Formation of Ions and Behavior of Electrolytes. Acid--Base Reactions in Non--Aqueous Solvents. Redox Reactions in Non--Aqueous Solvents. PART II: ELECTROCHEMICAL TECHNIQUES AND THEIR APPLICATIONS IN NON--AQUEOUS SOLUTIONS. Overview of Electrochemical Techniques. Potentiometry in Non--Aqueous Solutions. Conductimetry in Non--Aqueous Solutions. Polarography and Voltammetry in Non--Aqueous Solutions. Other Electrochemical Techniques in Non--Aqueous Solutions. Purification of Solvents and Tests for Impurities. Selection and Preparation of Supporting Electrolytes. Use of Non--Aqueous Solutions in Modern Electrochemical Technologies. Index.
  • (source: Nielsen Book Data)9783527305162 20160527
Nonaqueous solutions are equally indispensable to electrochemistry. Here, Kosuke Izutsu brilliantly illustrates the numerous aspects of this fascinating topic, whether the focus be on physicochemical processes or analytical methods. The author discusses solvation and solvent effects emphasizing dynamic aspects, important reactions including ionic and supercritical media, as well as advanced techniques in polarography and voltammetry. Throughout, he effortlessly manages to provide a comprehensive overview while also presenting the very latest developments. A number of example applications further enhance the practical value of this book and give it the feel of a reference work. Written for both users and specialists, this volume represents a wealth of vital information and belongs on every bookshelf.
(source: Nielsen Book Data)9783527305162 20160527
Science Library (Li and Ma)
CHEM-174-01, CHEM-274-01
Book
xxi, 833 p. : ill. ; 26 cm.
  • Major Symbols. Standard Abbreviations. Introduction and Overview of Electrode Processes. Potentials and Thermodynamics of Cells. Kinetics of Electrode Reactions. Mass Transfer by Migration and Diffusion. Basic Potential Step Methods. Potential Sweep Methods. Polarography and Pulse Voltammetry. Controlled--Current Techniques. Method Involving Forced Convention--Hydrodynamic Methods. Techniques Based on Concepts of Impedance. Bulk Electrolysis Methods. Electrode Reactions with Coupled Homogeneous Chemical Reactions. Double--Layer Structure and Adsorption. Electroactive Layers and Modified Electrodes. Electrochemical Instrumentation. Scanning Probe Techniques. Spectroelectrochemistry and Other Coupled Characterization Methods. Photoelectrochemistry and Electrogenerated Chemiluminescence. Appendix A: Mathematical Methods. Appendix B: Digital Simulations of Electrochemical Problems. Appendix C: Reference Tables. Index.
  • (source: Nielsen Book Data)9780471043720 20160528
This edition is fully revised to reflect the current state off the field. Significant additions include ultramicroelectrodes, modified electrodes, and scanning probe methods. Many chapters have been modified and improved, including electrode kinetics, voltammetric methods, and mechanisms of coupled chemical reactions.
(source: Nielsen Book Data)9780471043720 20160528
Science Library (Li and Ma)
CHEM-174-01
Book
xi, 401 p. : ill. ; 24 cm.
  • 1 Electrochemical Oxidation and Reduction of Organic Compounds: General Technique-- Anode and Cathode Materials-- Kinetics of Electron Transfer-- Analytical and Spectroscopic Techniques-- Pulse Radiolysis. 2 Oxidation of Alkanes, Haloalkanes and Alkenes: Radical-Cations-- Oxidation of Alkanes-- Oxidation of Haloalkanes-- Oxidation of Alkenes-- Intramolecular Cyclization-- Electrochemically Generated Reagents for Alkenes. 3 Alkenes and Phenylalkenes: Alkene Radical-Anions as Nucleophiles-- Activated Alkenes - Introduction-- Activated Alkenes - Dimerization in Aprotic Media-- Activated Alkenes - Dimerization in Protic Media-- B-Unsaturated Aldehydes and Ketones-- Intramolecular Cyclization-- Mixed Hydrocoupling Reactions-- Asymmetric Reduction-- Electrocatalytic Hydrogenation. 4. Reductive Bond Cleavage Processes - I: Dissociative Electron Transfer-- Reduction of Alkyl and Benzyl Halides-- Reactions of the Trichloremethyl Group-- Reductive Cyclization of B-Dihaloalkanes-- Alkenes from 1,2-Dibromides and Related Compounds-- Reduction of Aryl Halides-- Electrochemically Induced SRN1 Reaction-- Electrochemically Induced Radical Cyclization Reactions of Aryl Halides-- Carbon-Halogen Bond Reactions Catalysed by the Anode Material-- Carbon-Halogen Bond Reactions Catalysed by Ni, Co and Pd Complexes-- Reactions with Carbon Dioxide.
  • (source: Nielsen Book Data)9780444720078 20160528
Electrochemical reactions make significant contributions to organic synthesis either in the laboratory or on an industrial scale. These methods have the potential for developing more "green" chemical synthesis. Over recent years, modern investigations have clarified the mechanisms of important organic electrochemical reactions. Progress has also been made in controlling the reactivity of intermediates through either radical or ionic pathways. Now is the time to gather all the electrochemical work into a textbook. As an essential addition to the armory of synthetic organic chemists, electrochemical reactions give results not easily achieved by many other chemical routes. This book presents a logical development of reactions and mechanisms in organic electrochemistry at a level suited to research scientists and final year graduate students. It forms an excellent starting point from which synthetic organic chemists, in both academia and industry, can appreciate uses for electrochemical methods in their own work. The book is also a reference guide to the literature.
(source: Nielsen Book Data)9780444720078 20160528
Science Library (Li and Ma)
CHEM-174-01, CHEM-274-01

11. Electrode dynamics [1996]

Book
83 p. : ill. ; 25 cm.
  • 1. Introduction-- 2. Mass transport-- 3. Voltammetry: the study of electrolysis mechanisms-- 4. Structure of the electrode/solution interface-- 5. Spectroelectrochemistry.
  • (source: Nielsen Book Data)9780198556909 20160528
This highly illustrated textbook provides a framework of the key concepts involved in electrochemical kinetics. A wide range of modern electrochemical techniques and applications are discussed. The mathematical content has been minimised for clarity, whilst retaining the important results necessary for physical insight. A substantial series of examples and illustrations are taken from the recent research literature to explore the potential applications of electrochemical techniques. This book will be of interest to students taking courses in chemistry, material science, and physics students.
(source: Nielsen Book Data)9780198556909 20160528
Science Library (Li and Ma)
CHEM-174-01, CHEM-274-01